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|Title:||A Practical One-Pot Two-Step Protocol for the Microwave-Assisted Synthesis of Highly Functionalized Rhodanine Derivatives||Authors:||Radi, Marco
|Issue Date:||2010||Project:||None||Journal:||JOURNAL OF COMBINATORIAL CHEMISTRY||Abstract:||
A fast and efficient protocol for the generation of substituted 5-arylidene rhodanines in a sequential one-pot two-step process combining the “Holmberg method” and the Knoevenagel condensation under microwave-assisted conditions has been developed. The final compounds 11a−k have been obtained in high yield and purity after a simple precipitation from methanol, making this procedure facile, practical, and rapid to execute.
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