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|Title:||Rapid microwave-assisted deprotection of N-Cbz and N-Bn derivatives||Authors:||M. C., Daga
|Issue Date:||2001||Project:||None||Journal:||TETRAHEDRON LETTERS||Abstract:||
Catalytic-transfer hydrogenation in ifo-propanol under microwave irradiation has been performed to rapidly deprotect N-Cbz and N-Bn derivatives. The method is particularly suitable for the synthesis of short peptides and can also be carried out on supported molecules. The rapid cleavage of chiral molecules derived from (S)-1-phenylethylamine can be very useful for asymmetric synthesis of nitrogen containing compounds. (C) 2001 Elsevier Science Ltd. All rights reserved.
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