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|Title:||The Barton radical decarboxylation on solid phase. A versatile synthesis of peptides containing modified amino acids||Authors:||M. E., Attardi
|Issue Date:||2001||Project:||None||Journal:||TETRAHEDRON LETTERS||Abstract:||
Barton esters were prepared starting from different carboxylic acids loaded on a Wang resin. Light induced fragmentation occurred giving a radical that reacted with CBrCl3 to give the corresponding bromides, whereas conjugate addition to electron-poor alkenes proved to be less synthetically useful. The bromides so formed were further functionalised on the resin with different nucleophiles. (C) 2001 Elsevier Science Ltd. All rights reserved.
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